Comparison of essential oil and Oleoresin extractions from star anise fruits (Illicium verum H.) with liquid carbon dioxide, chemical solvents and by steam distillation (Record no. 19923)

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005 - DATE AND TIME OF LATEST TRANSACTION
control field 20260817173439.0
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION
fixed length control field 080598 th eng
035 ## - SYSTEM CONTROL NUMBER
System control number .b10151916
099 #9 - LOCAL FREE-TEXT CALL NUMBER (OCLC)
Classification number AIT Thesis no. AE-93-20
100 1# - MAIN ENTRY--PERSONAL NAME
Personal name Dang, Quoc Tuan
245 10 - TITLE STATEMENT
Title Comparison of essential oil and Oleoresin extractions from star anise fruits (Illicium verum H.) with liquid carbon dioxide, chemical solvents and by steam distillation
260 ## - PUBLICATION, DISTRIBUTION, ETC.
Place of publication, distribution, etc. Bangkok :
Name of publisher, distributor, etc. Asian Institute of Technology,
Date of publication, distribution, etc. 1993
300 ## - PHYSICAL DESCRIPTION
Extent 119 leaves :
Other physical details ill.
490 1# - SERIES STATEMENT
Series statement Thesis ;
Volume/sequential designation no. AE-93-20
502 ## - DISSERTATION NOTE
Dissertation note Thesis (M. Eng.) - Asian Institute of Technology, 1993
500 ## - GENERAL NOTE
General note A thesis submitted in partial fulfillment of the requirement for the degree of Master of Engineering.
520 ## - SUMMARY, ETC.
Summary, etc. Two methods to extract essential oil from dried Star anise fruits (Illicium verum Hook) namely steam distillation and liquid CO 2 extraction, and one method of oleoresin extraction using conventional solvents, were studied and the physic:;tl and chemical properties of Star anise essential oil such as color, specific gravity, refractive index, optical rotation and anethole content were determined. The yield of essential oil by st~am distillation was 10.4 mL/lOOg of the raw material having an initial moisture content of 12.7% (w.b.) and the rate of distillation was dependent on particle size of Star anise fruit powder. The recommended particle size and time for steam distillation was 0.57 mm and 1.5 h., respectively. The modified Lentz's apparatus for liquid co 2 extraction had a working pressure of 6.5 MPa for liquid CO. The yield of essential oil by liquid co extraction was dependent on particfe size, while the working pressure was kepf constant. The recommended particle size for liquid co 2 extraction is 0.57 mm. The essential oil yield by liquid co2 was 9% higher than that of steam distillation. The Langmuir's adsorption model was used to fit the experimental data of the liquid co 2 extraction yield. The same model was used to describe the anethole yield of extraction. Four types of solvents, i.e. analytical grade and commercial ethanol, analytical grade and commercial hexane, were tested for oleoresin extraction. Commercial ethanol was best while hexane was poor as a solvent for oleoresin extraction. The extraction rate with ethanol w'as dependent on heat intensity and particle size. The extraction rate exhibited two phases of extraction. An initial linear period described by simple linear function was followed by an increased period which was described by an exponential function. A similar pattern of extraction was observed for anethole yield. The recommended time and particle size for ethanol extraction was 4 h and 0.57 mm, respectively. The energy consumption analysis shows that the energy consumed for ethanol extraction was highest while energy consumption for liquid CO extraction was the lowest. The energy required for ethanol extraction was 6.J times higher than the energy required for liquid co 2 extraction and the energy required for steam distillation was 5. 9 times higher than that of liquid co2 extraction (based on 1 kg of the essential oil).
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Food
General subdivision Analysis
700 1# - ADDED ENTRY--PERSONAL NAME
Personal name Ilangantileke, S.G.,
Relator term Chairperson
700 1# - ADDED ENTRY--PERSONAL NAME
Personal name Jindal, Vinod Kumar,
Relator term Examination Committee
700 0# - ADDED ENTRY--PERSONAL NAME
Personal name Athapol Noomhorm,
Relator term Examination Committee
700 1# - ADDED ENTRY--PERSONAL NAME
Personal name Reutergardh, L.,
Relator term Examination committee
700 1# - ADDED ENTRY--PERSONAL NAME
Personal name Vincent, Jean Claude,
Relator term Examination committee
710 2# - ADDED ENTRY--CORPORATE NAME
Corporate name or jurisdiction name as entry element The Government of Germany (DAAD),
Relator term Scholarship donor
810 2# - SERIES ADDED ENTRY--CORPORATE NAME
Corporate name or jurisdiction name as entry element Asian Institute of Technology.
Title of a work Thesis ;
Volume/sequential designation no. AE-93-20
856 ## - ELECTRONIC LOCATION AND ACCESS
Materials specified Full-Text
Uniform Resource Identifier <a href="http://203.159.5.9/ait-thesis/detail.php?q=B16019">http://203.159.5.9/ait-thesis/detail.php?q=B16019</a>
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998 ## - LOCAL CONTROL INFORMATION (RLIN)
Operator's initials, OID (RLIN) 2
Cataloger's initials, CIN (RLIN) 951012
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945 ## - LOCAL PROCESSING INFORMATION (OCLC)
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942 ## - ADDED ENTRY ELEMENTS (KOHA)
Koha item type 20-AIT Publication
942 ## - ADDED ENTRY ELEMENTS (KOHA)
Koha item type 40-Archives
909 ## - LOCAL ITEMS USED
Barcode Barcode : 30050003008785
CREATED CREATED : 1994-05-16
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LCHKIN LCHKIN : 2001-07-23
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Barcode Barcode : 30050120375828
CREATED CREATED : 2016-01-06
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      Available for Loans Asian Institute of Technology Library Asian Institute of Technology Library AIT Publications 17/08/2026   AIT Thesis no. AE-93-20 30050003008785 17/08/2026 1 17/08/2026 20-AIT Publication
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