Development of an automatic electrochemical flow system for high throughput determination of total antioxidant capacity in biological materials (Record no. 29100)

MARC details
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005 - DATE AND TIME OF LATEST TRANSACTION
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008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION
fixed length control field 190827s2017 th uu m rtt 0| a1eng d
035 ## - SYSTEM CONTROL NUMBER
System control number .b12310086
099 ## - LOCAL FREE-TEXT CALL NUMBER (OCLC)
Classification number AIT Thesis no.FB-17-07
100 0# - MAIN ENTRY--PERSONAL NAME
Personal name Kornautchaya Veenuttranon
245 10 - TITLE STATEMENT
Title Development of an automatic electrochemical flow system for high throughput determination of total antioxidant capacity in biological materials
260 ## - PUBLICATION, DISTRIBUTION, ETC.
Place of publication, distribution, etc. Pathum Thani, Thailand :
Name of publisher, distributor, etc. Asian Institute of Technology,
Date of publication, distribution, etc. 2017
300 ## - PHYSICAL DESCRIPTION
Extent 90 leaves :
Other physical details ill. +
Accompanying material 1 online resource
490 1# - SERIES STATEMENT
Series statement Thesis ;
Volume/sequential designation no.FB-17-07
500 ## - GENERAL NOTE
General note A thesis submitted in partial fulfillment of the requirements for the degree of Master of Engineering in Food Engineering and Bioprocess Technology, School of Environment, Resources and Development
502 ## - DISSERTATION NOTE
Dissertation note Thesis (M. Sc.) - Asian Institute of Technology, 2017
520 ## - SUMMARY, ETC.
Summary, etc. The aim of this work was to develop a programmable compressed - nitrogen gas flow system combined with electrochemical based assay for assessment of total antioxidant capacity (TAC) using the 2, 2 - diphenyl - 2 - picrylhydrayl hydrate (DPPH{u2022}) solution as a redox indicator on a screen printed carbon electrode ( SPE) . Gallic acid (GA) was chosen as a standard antioxidant. Firstly , the prototype device was designed and fabricated with an internal volume of 1,500 oL . A programmable electronic controlled 3 - way solenoid valve was utilized to control the liquid flow and retention time inside the reaction chamber of the system. A suitable driven pressure for compressed nitrogen gas was 20 kPa which was used to control the volumetric dosage of samples and reagents. There were a good linear relationship between propelled time and volumetric dosage (R 2 > 0.999 ) for all injection ports in which the linear regression equations were used to determine an accurate time for liquid injection . T he electrochemical characterizations of DPPH{u2022} and GA were performed using cyclic voltammetry (CV) , as a result, a suitable applied potential (E) of - 0.05 V was select ed for amperometric determination of TAC. The calibration curve was developed by measuring the constant currents of amperometry ( I ) for different concentration of GA in fixed 0.05 mM DPPH solution, after incubating the mixture for 2 min. One pure compound of ascorbic acid and four liquid food samples (orange juice, pomegranate juice, white wine and green tea) were mixed instead of GA and respective ( I ) were measured to determine the TAC. The results of TAC was then expressed in terms of gallic acid equivalent antioxidant capacity (GEAC). All the above experiments were co - conducted with the spectrophotometric analysis and results were compared. A good linear correlation (R 2 = 0.996 ) was obtained between electrochemical test within flow mixing system and conventional method of DPPH{u2022} scavenged by ascorbic acid, and two methods could be used interch ange (slope = 0.951 ). IC 50 and TAC of four samples were investigated by dif ferentiating the concentration and there was no significant difference (p> 0. 05) between the two methods.
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Antioxidants
General subdivision Biotechnology
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Biomaterials
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Electrochemical apparatus
700 1# - ADDED ENTRY--PERSONAL NAME
Personal name Loc Thai Nguyen,
Relator term Chairperson
700 1# - ADDED ENTRY--PERSONAL NAME
Personal name Anal, Anil Kumar,
Relator term Examination Committee
700 1# - ADDED ENTRY--PERSONAL NAME
Personal name Sadiq, Muhammad Bilal,
Relator term Examination committee
710 2# - ADDED ENTRY--CORPORATE NAME
Corporate name or jurisdiction name as entry element RTG Fellowship,
Relator term Scholarship donor
810 2# - SERIES ADDED ENTRY--CORPORATE NAME
Corporate name or jurisdiction name as entry element Asian Institute of Technology.
Title of a work Thesis ;
Volume/sequential designation no. no.FB-17-07
856 ## - ELECTRONIC LOCATION AND ACCESS
Materials specified Full-Text
Uniform Resource Identifier <a href="http://203.159.5.9/ait-thesis/detail.php?q=B02864">http://203.159.5.9/ait-thesis/detail.php?q=B02864</a>
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998 ## - LOCAL CONTROL INFORMATION (RLIN)
Operator's initials, OID (RLIN) 0
Cataloger's initials, CIN (RLIN) 190827
First date, FD (RLIN) m
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Koha item type 40-Archives
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Koha item type 61-CD-ROM
942 ## - ADDED ENTRY ELEMENTS (KOHA)
Koha item type 20-AIT Publication
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      Available for Loans Asian Institute of Technology Library Asian Institute of Technology Library Archives 18/08/2026   AIT Thesis no.FB-17-07 30050120894406 18/08/2026 1 18/08/2026 40-Archives  
      Available for Loans Asian Institute of Technology Library Asian Institute of Technology Library Archives 18/08/2026   AIT Thesis no.FB-17-07   18/08/2026   18/08/2026 61-CD-ROM  
      Available for Loans Asian Institute of Technology Library Asian Institute of Technology Library AIT Publications 18/08/2026   AIT Thesis no.FB-17-07 30050120955470 18/08/2026 1 18/08/2026 20-AIT Publication 50.00
      Available for Loans Asian Institute of Technology Library Asian Institute of Technology Library AIT Publications 18/08/2026   AIT Thesis no.FB-17-07 30050120955447 18/08/2026 2 18/08/2026 20-AIT Publication 50.00
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